Part | NASKA2 (LC)-Triple Quad 4500 (MS/MS) | ||
---|---|---|---|
Column | Osaka Soda Capcell pak C18 (4.6 mm × 35 mm, 5 | ||
Injection volume | 5 | ||
Mobile phase | A : 5 mM Ammonium formate in water | ||
Oven temp. | Time (min) | A (%) | B (%) |
0.00 | 75.0 | 15.0 | |
1.00 | 75.0 | 15.0 | |
1.50 | 30.0 | 60.0 | |
10.00 | 10.0 | 90.0 | |
15.00 | 10.0 | 90.0 | |
20.00 | 2.0 | 98.0 | |
20.10 | 75.0 | 15.0 | |
Flow rate | 0.25 mL/min | ||
Oven temp. | 40°C | ||
Ion source | ESI (electrospray ionization) |